Another surface problem is tackled by Richard Pilkington, Stuart Astin and John Cowpe: “Application of laser-induced breakdown spectroscopy for surface hardness measurements”. Measuring the hardness of materials is not entirely straightforward, and the authors show that laser-induced breakdown spectroscopy offers the potential for in situ hardness measurements, without prior sample preparation.
Frank Rutten, Jasim Jamur and Paul Roach tell us about another: “Fast and versatile ambient surface analysis by plasma-assisted desorption/ionisation mass spectrometry”. They show that surface analysis can greatly benefit from approaches using surface–plasma interactions and that PADI shows significant promise to become a valuable and versatile tool for this.
To ensure that the removal and treatment of our sewerage meets increasingly high standards, it is important to be able to monitor the water online both to provide timely information and also to establish changing patterns over days, weeks and seasons. In their article “On-line monitoring for improved wastewater system management: applications of ultraviolet/visible spectroscopy”, Rita Brito, Rita Ribeiro, Tatiana Arriaga, Catarina Leitão, Nìdia Lourenço, Filipa Ferreira and Helena Pinheiro demonstrate the value of on-line UV/vis spectroscopy for wastewater quality monitoring in decentralised wastewater treatment and for spectral on-line monitoring of key quality parameters at the inlet to wastewater treatment plants.
In the Tony Davies Column, Tony looks at “Raman imaging of difficult surfaces”. He looks at a number of different approaches to dealing with uneven samples, as well as reviewing instrumental improvements that have made Raman imaging a viable analytical and diagnostic tool.
In the Quality Matters Column, Peter Jenks, Paul Boother and Annette Marshall are concerned about “The proper use of certified reference materials for analytical instrumentation qualification”. There are many aspects to consider in ensuring the validity of an analytical system, from before any instrumentation is installed, before it is used and during its use. Readers interested in the chemicals and reference material field may be interested in the news that, as this issue was being prepared, Merck completed its $17-billion acquisition of Sigma-Aldrich.
Kim Esbensen and Claas Wagner’s Sampling Column also addresses issues around ensuring valid results, from the sampling perspective. “Composite sampling II: lot dimensionality transformation” continues to address the problem of heterogeneity and how to overcome it. If you can find a time when your bulk (3D) sample becomes a 1D sample, the job is possible. Interesting examples from unloading a grain ship to emptying a fishing boat hold are described.
Fine sediments, often due to run-off from the land, can clog the surface and sub-surface spaces in gravel beds used by spawning fish to lay their eggs and by aquatic insects. Without an adequate flow of oxygenated water, the eggs and insects die. Heather Haynes, Susithra Lakshmanan, Anne-Marie Ockelford, Elisa Vignaga and William Holmes tells us about this in “The emerging use of magnetic resonance imaging to study river bed dynamics”. They have studied the infiltration of various sediments into model gravel beds both outside and flowing through a MRI instrument! They conclude that MRI “provides an exciting opportunity to unravel a plethora of processes relevant to wider environmental science”.
Graphene has been receiving a large amount of interest as its commercial possibilities begin to be realised. Now, with hundreds of companies offering commercial graphene production, analytical measures of graphene quality are required. Raman spectroscopy can be used to “understand the number of layers, strain, doping and importantly the level of disorder present in graphene”, which is described in this article: “Graphene characterisation and standardisation via Raman spectroscopy” by Andrew Pollard and Debdulal Roy.
- A new approach to identifying unknown trace level analytes by tandem mass spectrometry without reference spectroscopic database support: CSI:FingerID
- The analysis of poly aromatic compounds: a never-ending story?
- Composite sampling I: the Fundamental Sampling Principle
- Direct Analysis in Real Time mass spectrometry and its application for the analysis of polydimethylsiloxanes
Page 1 of 25
- Application of laser-induced breakdown spectroscopy for surface hardness measurements
- Fast and versatile ambient surface analysis by plasma-assisted desorption/ionisation mass spectrometry
- On-line monitoring for improved wastewater system management: applications of ultraviolet/visible spectroscopy
- The emerging use of magnetic resonance imaging to study river bed dynamics
Free print subscription
tesfaye saidthe NIR spectroscopy reduced the cost... 2 months ago
fred isaboke saidWant to inquire about the specificati... 9 months ago
Markus Rupprecht saidDear Tony Davies,
thank you so much f... 11 months ago
corriou saidI have read with interest the text, b... 1 year ago
Kim H. Esbensen saidre. WDXRF possibilities to map hetero... 1 year ago
- Atomic absorption
- Atomic emission
- Ion mobility
- Laser spectroscopy
- Mass spectrometry
- Near infrared
- NMR ESR EPR
- North America
- Related equipment
- RMs and standards
- Separation science
- South America
- Surface analysis
- X-ray spectrometry